Thermal analysis apparatus STA 449 F3 Jupiter

Trade name
Thermal analysis apparatus STA 449 F3 Jupiter Netzsch
Technical description

The apparatus allows thermal analysis of solid and powder samples in the range of RT-1500°C in an atmosphere of nitrogen, helium and technical air, along with gas analysis by QMS and FTIR.

Technical parameters:

• real measurement of TG, DTA-TG, DSC-TG

• temperature range RT ÷ 1500 °C (Pt furnace)

• dynamic measurement with the heating speed in the range of 0.01 ÷ 50 K/min

• in quasi-isothermal conditions

• maximum weight: 35 g

• registration of mass changes with an accuracy of 1µg (in the entire range)

• in an inert, oxidizing, reducing atmosphere and in a vacuum, in static or

  dynamic mode

Conditions for providing infrastructure

- according to the regulations listed on the laboratory's website: http://wydzlab.agh.edu.pl/wp-content/uploads/2020/11/Regulamin-WLBFSTiG.pdf
- scientific and research cooperation with AGH units and other domestic and foreign scientific units
- within the projects of NCN, NCBiR, cooperation with industry and under contracts

Type of accreditation / certificate:
Not applicable
Access type
External
Research capabilities

- testing of thermal stability and processes occurring during heating of solid mineral

- determination of the purity of crystalline substances

- studies of polymorphic transformations and thermal dissociation

- determination of process kinetics parameters

- determination of thermodynamic processes parameters

- qualitative analysis of pyrolytic gas products using QMS methods and FTIR TGA-IR

Last update date
June 10, 2023, 11:02 p.m.
Year of commissioning
2012
Measurement capabilities

Simultaneous measurement of STA and gaseous pyrolysis products using QMS methods and FTIR, - registration: QMS spectra in the range of 1 ÷ 300 m/z, - a set of FTIR spectra in the range of 4000-400 cm-1 during STA measurement: - extraction of the FTIR spectrum for the desired temperature, - generating variability of the intensity of the desired band, on FTIR spectra, as a function of temperature (temperature trace)

Photos
STA 449 F3 Jupiter Netzsch coupled with a QMS quadrupole mass spectrometer 403 C Aelos and a Bruker Tensor 27 FTIR spectrometer
STA 449 F3 Jupiter Netzsch coupled with a QMS quadrupole mass spectrometer 403 C Aelos and a Bruker Tensor 27 FTIR spectrometer