Pulsed Laser Deposition System

Trade name
Pioneer 180 PLD System
Technical description

The PLD system allows the fabrication of epitaxial films, multilayer heterostructures, superlattices, and amorphous layers from various materials (metals, nonmetals, oxides, ceramics, etc.) on a variety of substrates. Our system is equipped with a multi-target carousel with 6 places for different targets (1-inch in diameter), which makes it possible to produce multi-layered heterostructures (e.g. LSMO/BTO/LSMO, LAO/STO, etc.) in a single growth process.

Our PLD system consists of:

  • a loadlock for pre-pumping;
  • a main vacuum chamber with a base pressure of ~ 8E-8 Torr and the possibility to use gas atmospheres (oxygen, nitrogen, and argon) during the growth process;
  • UV eximer KrF laser 248nm COMPex 110F (pulse frequency 1 – 100 Hz, max power 200mJ);
  • RHEED measurement system by STIBE Instruments.

Substrates with a diameter of up to 2 inches can be used for the growth process. One of the sample holders is specifically designed for 10x10 mm substrates. The substrate can be continuously rotated during growth (1 - 30 rpm, 360°).

Growth can be performed in a temperature range from room temperature to 850 °C. The heating and cooling rates are digitally adjustable to within 1 °C/min. The radiative heater is compatible with oxygen up to 1 atm (760 Torr) of O2. It is mounted on top of the sample holder with the substrate surface facing the ground.

The RHEED technique is also compatible with oxygen up to ~ 1E-3 Torr of O2. The in-situ RHEED diagnostics enables the study of the crystal structure and growth kinetics of thin films. In addition, monitoring RHEED oscillations operando, i.e., during film growth, enables the control of layer thickness on the unit-cell level.

Conditions for providing infrastructure

Equipment is available in accordance with the Regulations for the Use of ACMiN's Research Infrastructure. (https://acmin.agh.edu.pl/home/acmin/5_Wspolpraca/Aparatura/Zasady_i_koszty_korzystania_z_infrastruktury_badawczej_ACMiN.pdf)

Type of accreditation / certificate:
Not applicable
Access type
External
Research capabilities

The laser ablation system makes it possible to obtain epitaxially layered samples with good thickness control through in-situ measurements using the RHEED method.

The RHEED method also allows testing of properly prepared samples for their crystallographic structure, as well as quality control of the microstructure after etching processes down to the atomic layer level.

Last update date
March 10, 2025, 1:36 p.m.
Year of commissioning
2013
Photos
Pulsed Laser Depositon System
Pulsed Laser Depositon System