DualBeam Ultra-high-resolution Scanning Electron Microscop with Xenon (Xe) Plasma Focused Ion Beam (PFIB/SEM) with Atomic Force Microscope (AFM)

Trade name
Thermo Fisher Scientific Helios 5 PFIB CXe
Technical description

Helios 5 is a double-beam ultra-high-resolution scanning electron microscope equipped with a high-stability Schottky Field Emission Gun (FEG) and a Plasma Focused Ion Beam (PFIB). It enables operation with accelerating voltage in the range from 350 V to 30 kV (max. electron beam current 100 nA), the landing energy range from 20 eV to 30 keV, and a resolution of 0.7 nm at 1 kV for a gold particle standard sample. Maximum horizontal field width is 2.3 mm at 4 mm WD.

The microscope is equipped with:

  • detectors: Elstar in-lens detector (TLD-SE, TLD-BSE); Elstar in-column detector (ICD - SE/BSE); Everhart-Thornley SE detector (ETD); retractable low voltage, high contrast directional solid-state backscatter electron detector (DBS); high-performance in-chamber electron and ion detector (ICE) for secondary ions (SI) and electrons (SE),
  • retractable STEM3+ detector with BF/DF/HAADF segments,
  • Ultim MAX 60 Energy Dispersive X-ray Spectrometer (EDS) and the Symmetry S3 CMOS camera by Oxford Instruments, enabling measurements of Electron Backscatter Diffraction (EBSD),
  • high-performance PFIB column with inductively coupled Xe+ Plasma and Gas Injection System (GIS). Possibility of platinum (Pt) and tungsten (W) deposition,
  • nanoindenter FT-NMT04 from FemtoTools,
  • Auto Slice&View software,
  • LiteScope AFM-in-SEM stage from NenoVision.

Maximum dimensions of samples – diameter: 110 mm, height: 65 mm; weight: 500g.

Conditions for providing infrastructure

Equipment is available in accordance with the Regulations for the Use of ACMiN's Research Infrastructure. (https://acmin.agh.edu.pl/home/acmin/5_Wspolpraca/Aparatura/Zasady_i_koszty_korzystania_z_infrastruktury_badawczej_ACMiN.pdf)

Type of accreditation / certificate:
Not applicable
Access type
External
Research capabilities
  1. High-resolution microstructural observations of conductive and non-conductive materials.
  2. Nanohardness measurements.
  3. Surface topography analysis (AFM).
  4. Electron tomography (SEM/PFIB) - 3D microstructure reconstruction.
  5. Analyzes of elemental composition (EDS).
  6. Crystallographic orientation analysis (EBSD).
  7. Highest quality Ga+ free TEM and APT sample preparation.
Last update date
March 10, 2025, 1:42 p.m.
Year of commissioning
2024
Measurement capabilities
  1. The size and shape analyses of particles and pores, thickness measurement of micro- and nanocoatings.
  2. STEM observations:
    • Bright Field (BF),
    • Dark Field (DF),
    • High-Angle Annular Dark Field (HAADF).
  3. Precise preparation of sample cross-sections using PFIB thanks to the Rocking Polish technique.
  4. Acquiring SEM images from large areas is possible thanks to Mapa 3 software.
Photos
Helios 5 (SEM/PFIB)
Helios 5 (SEM/PFIB)
AFM NenoVision
AFM NenoVision