DualBeam Ultra-high-resolution Scanning Electron Microscop with Xenon (Xe) Plasma Focused Ion Beam (PFIB/SEM) with Atomic Force Microscope (AFM)
Helios 5 is a double-beam ultra-high-resolution scanning electron microscope equipped with a high-stability Schottky Field Emission Gun (FEG) and a Plasma Focused Ion Beam (PFIB). It enables operation with accelerating voltage in the range from 350 V to 30 kV (max. electron beam current 100 nA), the landing energy range from 20 eV to 30 keV, and a resolution of 0.7 nm at 1 kV for a gold particle standard sample. Maximum horizontal field width is 2.3 mm at 4 mm WD.
The microscope is equipped with:
- detectors: Elstar in-lens detector (TLD-SE, TLD-BSE); Elstar in-column detector (ICD - SE/BSE); Everhart-Thornley SE detector (ETD); retractable low voltage, high contrast directional solid-state backscatter electron detector (DBS); high-performance in-chamber electron and ion detector (ICE) for secondary ions (SI) and electrons (SE),
- retractable STEM3+ detector with BF/DF/HAADF segments,
- Ultim MAX 60 Energy Dispersive X-ray Spectrometer (EDS) and the Symmetry S3 CMOS camera by Oxford Instruments, enabling measurements of Electron Backscatter Diffraction (EBSD),
- high-performance PFIB column with inductively coupled Xe+ Plasma and Gas Injection System (GIS). Possibility of platinum (Pt) and tungsten (W) deposition,
- nanoindenter FT-NMT04 from FemtoTools,
- Auto Slice&View software,
- LiteScope AFM-in-SEM stage from NenoVision.
Maximum dimensions of samples – diameter: 110 mm, height: 65 mm; weight: 500g.
Equipment is available in accordance with the Regulations for the Use of ACMiN's Research Infrastructure. (https://acmin.agh.edu.pl/home/acmin/5_Wspolpraca/Aparatura/Zasady_i_koszty_korzystania_z_infrastruktury_badawczej_ACMiN.pdf)
- High-resolution microstructural observations of conductive and non-conductive materials.
- Nanohardness measurements.
- Surface topography analysis (AFM).
- Electron tomography (SEM/PFIB) - 3D microstructure reconstruction.
- Analyzes of elemental composition (EDS).
- Crystallographic orientation analysis (EBSD).
- Highest quality Ga+ free TEM and APT sample preparation.
- The size and shape analyses of particles and pores, thickness measurement of micro- and nanocoatings.
- STEM observations:
- Bright Field (BF),
- Dark Field (DF),
- High-Angle Annular Dark Field (HAADF).
- Precise preparation of sample cross-sections using PFIB thanks to the Rocking Polish technique.
- Acquiring SEM images from large areas is possible thanks to Mapa 3 software.



Responsible body
Group / laboratory / team
Department of Functional Materials and Nanomagnetism